HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 70217235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | (2s)-Glycidyl indol-4-yl ether | HCID 10943254 | — |
| Reactant | HCID 18797335 | HCID 18797335 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 70217235 | HCID 70217235 | — |
Reaction Steps
The title compound was prepared in a fashion similar to that described in Example 1 using (S)-(+)-4-(oxiranylmethoxy)-1H-indole (0.075 g, 0.042 mmol), and 5-chloro-2-(1,2,3,6-tetrahydropyridin-4-yl)benzo[b]thiophene (0.100 g, 0.042 mmol) using ethanol as reaction solvent. Yield 0.103 g (58%) of an orange oil. FDMS m/e=438 (M+ of free base). α[D]589 =+7.3 (c=0.95, dimethylsulfoxide)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05627196 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-3f3d777a33d44158bd96de10a74a644f |
| Source note | uspto-grants-1997_05 |