HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 54309624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | HCID 54184811 | HCID 54184811 | — |
| Catalyst | chromium (VI) trioxide | HCID 10219390 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54309624 | HCID 54309624 | — |
Reaction Steps
Using the procedure described in Org. Syn., 1976, 55, 84, (3β,5α,11β,12α,25R)-3,12-di(acetoxy)-spirostan-11-ol was oxidized with chromium trioxide and pyridine in methylene chloride to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629295 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-6fa217724b66456e9d956f1b5c88ddee |
| Source note | uspto-grants-1997_05 |