HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Lutidine → HCID 53652232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Lutidine | HCID 7937 | — |
| Reactant | Trimethylsilyl triflate | HCID 65367 | — |
| Reactant | HCID 53967493 | HCID 53967493 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53652232 | HCID 53652232 | — |
Reaction Steps
(3β,5α,11β,12β,25R)-3-(t-butyldimethylsilyloxy)-12-acetoxyspirostan-11-ol was silylated with trimethylsilyltriflate and 2,6-lutidine in methylene chloride according to the procedure described in Tetrahedron Letters, 1981, 22, 3455.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629295 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-7a3b214cc6ab4fca8e52a0c92fb0f350 |
| Source note | uspto-grants-1997_05 |