L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]- → HCID 67689621, compound

HRID 1780218Notes

Reaction equation

HRID 1780218 reaction equation
Cl.[NH2:2][CH2:3][P:4]([CH2:7][NH2:8])(=[O:6])[OH:5].[C:9]([O:13][C:14]([NH:16][C@H:17]([C:25]([OH:27])=O)[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:15])([CH3:12])([CH3:11])[CH3:10]>>[C:9]([O:13][C:14]([NH:16][C@H:17]([C:25]([CH:3]([P:4]([CH:7]([NH2:8])[C:25](=[O:27])[C@H:17]([CH2:18][C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1)[NH:16][C:14]([O:13][C:9]([CH3:10])([CH3:11])[CH3:12])=[O:15])(=[O:5])[OH:6])[NH2:2])=[O:27])[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)=[O:15])([CH3:11])([CH3:12])[CH3:10]

Participants

3

Reactant 2

HCID 77857L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]-HCID 12565359HCID 12565359, compound

Product 1

HCID 67689621HCID 67689621, compound

Procedure

Synthesis in analogy to Example 1 from bis(aminomethyl)phosphinic acid hydrochloride and tert.-butoxycarbonyI-L-phenylalanine

Sources & evidence

ORD record
ord-55c9be79ba4b474ab4247261956eb64d
Source dataset
uspto-grants-1997_05
Patent number
US05629431

Reaction notes

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