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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1780256Generated: November 1, 2026

(2S,3S)-3-(N2-benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid → HCID 473124, compound

https://huagongshe.com/reaction/1780256

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(2S,3S)-3-(N2-benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acidHCID 57125825—
ReactantHCID 67722501HCID 67722501—
ProductHCID 473124HCID 47312424%

Reaction Steps

Following a procedure similar to that described in Example 1, but using 146 mg (0.33 mmol) of (2S,3S)-3-(N2 -benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid and 100 mg (0.33 mmol) of (4R)-N-t-butoxycarbonyl-4-chloro-N-t-butyl-L-prolinamide, 50 mg of the title compound were obtained as a colorless powder, melting at 103°-107° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05629406
Source datasetuspto-grants-1997_05
ORD IDord-956a064bfc1a4577afbf77842018bceb
Source noteuspto-grants-1997_05