HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S,3S)-3-(N2-benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid → HCID 473124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S,3S)-3-(N2-benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid | HCID 57125825 | — |
| Reactant | HCID 67722501 | HCID 67722501 | — |
| Product | HCID 473124 | HCID 473124 | 24% |
Reaction Steps
Following a procedure similar to that described in Example 1, but using 146 mg (0.33 mmol) of (2S,3S)-3-(N2 -benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid and 100 mg (0.33 mmol) of (4R)-N-t-butoxycarbonyl-4-chloro-N-t-butyl-L-prolinamide, 50 mg of the title compound were obtained as a colorless powder, melting at 103°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629406 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-956a064bfc1a4577afbf77842018bceb |
| Source note | uspto-grants-1997_05 |