HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 70048814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 67722739 | HCID 67722739 | — |
| Product | HCID 70048814 | HCID 70048814 | 91.5% |
Reaction Steps
Following a procedure similar to that described in Example 67, but using 500 mg (1.01 mmol) of 1-[3-(L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-N-t-butyl-L-prolinamide hydrochloride and 123 μl (1.21 mmol) of benzaldehyde, 510 mg of the title compound were obtained as a colorless powder, melting at 96°-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629406 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-b30681c7f9ad47c5a8431652835701fa |
| Source note | uspto-grants-1997_05 |