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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1780268Generated: November 2, 2026

HCID 57010663, compound → HCID 70058296, compound

https://huagongshe.com/reaction/1780268

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57010663HCID 57010663—
Reactant(2S,3S)-3-(N2-benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acidHCID 57125825—
ProductHCID 70058296HCID 7005829665.3%

Reaction Steps

79 mg (0.24 mmol) of N-benzyloxycarbonyl-N-(1,1-dimethyl-2-hydroxypropyl)-L-prolinamide were subjected to debenzyloxycarbonylation in a similar manner to that described in Example 17, and then the resulting product was condensed with 106 mg (0.24 mmol) of (2S,3S)-3-(N2 -benzyloxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyric acid in a similar manner to that described in Example 1, to give 98 mg of the title compound as a colorless powder, melting at 102°-104° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05629406
Source datasetuspto-grants-1997_05
ORD IDord-fb2a2a17208942e7a8240f8afc3caa61
Source noteuspto-grants-1997_05