Lead diacetate trihydrate → Lead diacetate

Participants

Reaction Steps

A 11.65-g portion of lead acetate trihydrate was added to 75 g of 2-methoxyethanol, and the resulting mixture was heated to dissolution for dehydration as an azeotropic mixture thereby providing a solution of anhydrous lead acetate. To this solution there were added 6.12 g of zirconium tetra-n-butoxide, 4.19 g of titanium tetra-isopropoxide and 2-methoxyethanol in an amount required to adjust the total weight of the mixture to 100 g thereby providing a 10% by weight solution of PbZr0.52 Ti0.48 O3 (PZT), and 2-nitrobenzyl alcohol was added thereto in each of the proportions indicated in TABLE 1 to provide compositions for formation of PZT thin-film patterns.

Provenance & Evidence