Lead diacetate trihydrate → Lead diacetate

Participants

Reaction Steps

A 11.65-g portion of lead acetate trihydrate was added to 75 g of 2-methoxyethanol, and the resulting mixture was heated to dissolution for dehydration as an azeotropic mixture thereby providing a solution of anhydrous lead acetate. To this solution there were added 6.12 g of zirconium tetra-n-butoxide, 4.19 g of titanium tetra-isopropoxide and 2-methoxyethanol in an amount required to adjust the total weight of the mixture to 100 g thereby providing a 10% by weight PbZr0.52 Ti0.48 O3 (PZT) composition for formation of thin films. A 4.7 g-portion of 2-nitrobenzyl alcohol was added to the composition to provide a composition for formation of photosensitive PZT thin-film patterns. This composition was then diluted to ten-fold with 2-methoxyethanol to prepare a solution for LSMCVD.

Provenance & Evidence