HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19047208, compound → HCID 23298800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19047208 | HCID 19047208 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23298800 | HCID 23298800 | 89.9% |
Reaction Steps
At the same time, 11-trimethylsilyl-10-undecynoic acid (0.23 g) was dissolved in ethyl acetate (5 ml), and 10% palladium-carbon (10 mg) was added to the solution. After the air within the reactor was purged with hydrogen, the mixture was stirred at room temperature for 12 hours. Then, the mixture was filtered, and the filtrate was concentrated to give 11-trimethylsilylundecanoic acid (0.21 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631238 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-a84d1f355c03410da2b6036f00decac0 |
| Source note | uspto-grants-1997_05 |