Thionyl Chloride → 3-(1-Octyloxycarbonyl)-2,2-dimethylbutyric acid chloride

HRID 1780932Notes

Reaction equation

HRID 1780932 reaction equation
[CH2:1]([O:9][C:10]([CH:12]([CH3:19])[C:13]([CH3:18])([CH3:17])[C:14](O)=[O:15])=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:22])=O>>[CH2:1]([O:9][C:10]([CH:12]([CH3:19])[C:13]([CH3:18])([CH3:17])[C:14]([Cl:22])=[O:15])=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19047496HCID 19047496, compound

Product 1

HCID 538993653-(1-Octyloxycarbonyl)-2,2-dimethylbutyric acid chloride

Procedure

3-(1-Octyloxycarbonyl)-2,2-dimethylbutyric acid (0.4 g) was treated with thionyl chloride (20 ml) and the excess thionyl chloride was removed in vacuo to afford 0.33 g of 3-(1-octyloxycarbonyl)-2,2-dimethylbutyric acid chloride.

Workup

  1. customthe excess thionyl chloride was removed in vacuo

Sources & evidence

ORD record
ord-6956540df8cc4043ada703c4bf8c5ec1
Source dataset
uspto-grants-1997_05
Patent number
US05631264

Reaction notes

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