Sodium Hydroxide → HCID 131720018, compound

HRID 1780943Notes

Reaction equation

HRID 1780943 reaction equation
[OH-].[Na+].C([O:6][C:7](=[O:53])[CH:8]([NH:31][C@H:32]([C@@H:35]([C@@H:37]([CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH3:52])[OH:38])[OH:36])[CH2:33][OH:34])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])(=O)C>C(O)C>[OH:53][C:7](=[O:6])[CH:8]([NH:31][C@H:32]([C@@H:35]([C@@H:37]([CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH3:52])[OH:38])[OH:36])[CH2:33][OH:34])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]

Participants

4

Reactant 2

HCID 14798Sodium Hydroxide2×HCID 131720019HCID 131720019, compound

Product 1

HCID 131720018HCID 131720018, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Sodium hydroxide (0.08 ml, 6.18M) is added to a stirred solution of 58 mg of N-(α-acetoxy-tetracosanoyl) phytosphingosine in 3 ml of 96% ethanol. After 1.5 hours, additional 6.18M sodium hydroxide (0.05 ml) is added and stirring is continued for 0.5 hour.

Workup

  1. waitis continued for 0.5 hour

Sources & evidence

ORD record
ord-5e431815bfc34fb79e4253adb29aeeb3
Source dataset
uspto-grants-1997_05
Patent number
US05631356

Reaction notes

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