HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-[(1S,2S,3R)-2,3-Dihydroxy-1-(hydroxymethyl)heptadecyl]octadecanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 86750847 | HCID 86750847 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-[(1S,2S,3R)-2,3-Dihydroxy-1-(hydroxymethyl)heptadecyl]octadecanamide | HCID 9898642 | — |
Reaction Steps
The above-described solution is added as quickly as possible to a suspension of 6.2 kg (13.9 moles) of phytosphingosine sulphate (purity of 82%) in 20 l methylene chloride and 2.8 l (20 moles) triethyl amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631356 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-7cc298cf86454962bef9fbda0eabf8c4 |
| Source note | uspto-grants-1997_05 |