Tris(2-aminoethyl)amine → HCID 22741549, compound

Participants

Reaction Steps

1H NMR (300 MHz,in CDCl3): δ2.71 (t,J=6 Hz,4H,-N-CH2 -CH2 -N(CH3)-), 2.64 (s,4H,-N-CH2 -C(CH3)2-S-), 2.62 (t,J=6 Hz,4H,-N-CH2 -CH2 -N(CH3)-), 2.52 (m,2H,-CH2 -CH2 -N(CH3)2), 2.46 (m,2H,-CH2 -CH2 -N(CH3 (2), 2.37 (s,6H,-CH2 -N(CH3)-CH2 -), 2.25 (s,6H,-CH2 -CH2 -N(CH3)2) and 1.28 (s,12H,-S-C(CH3)2 -) ppm. 13C NMR (75 MHz, in CDCl3): δ74.8, 67.7, 57.6, 57.2, 53.9, 51.7, 51.3, 45.9, 45.1 and 26.9 ppm. MS (El; m/z): 376(4,M+), 377(2,M+ +1), 378(0.6,M+ +2), 318(1,M+ -((CH3)2N-CH2 ·)), 262 (3), 255 (1), 246(1), 187 (7), 156(9), 144(8), 133(9), 130(16), 113 (17), 101(27), 99(21), 98(12), 72(32), 71(28), 70(42), 58(100), 56(13), 55(13), 43(31), and 42(38).

Provenance & Evidence