HCID 54199685, compound → HCID 53999362, compound

Participants

Reaction Steps

Compound 41 (52 mg, 0.053 mmol) was hydrogenated as described for the preparation of 44 to provide 61 (25 mg, 89.2%) as a white powder after lyophilization; [α]D +115 (c 0.28, water); 1H-n.m.r. (D2O): δ5.20(d, 1H, J1',2' 3.8 Hz, H-1'), 5.13(d, 1H, J1,2 3.8 Hz, H-1), 3.75, 3.46(s, 3H each, 2×OCH3) 2.39(t, 2H J 7.5 Hz, CH2COO).

Provenance & Evidence