Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl ester → Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]acetyl]-2,4,6-tris(1-methylethyl)phenylester

HRID 1781453Notes

Reaction equation

HRID 1781453 reaction equation
[CH3:1][CH:2]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])[CH3:3].S(=O)(=O)(O[C:36]1[C:41](C(C)C)=CC=C[C:37]=1C(C)C)N.S(=O)(=O)(OC1C(C(C)C)=CC(C(C)C)=CC=1C(C)C)N>>[CH3:3][CH:2]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:11])[CH3:12])[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][C:21]=1[CH:36]([CH3:41])[CH3:37])=[O:15])[CH3:1]

Participants

4

Reactant 3

HCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 153425652,6-Di(propan-2-yl)phenyl sulfamateHCID 232090992,4,6-Triisoproplyphenyl sulfamate

Product 1

HCID 10164046Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]acetyl]-2,4,6-tris(1-methylethyl)phenylester

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisoproplyphenyl sulfamate was replaced with 2,4,6-triisoproplyphenyl sulfamate, mp 152°-155° C.

Sources & evidence

ORD record
ord-3b4d52e0b1ee4171bff7d7d670e8bc53
Source dataset
uspto-grants-1997_05
Patent number
US05633287

Reaction notes

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