2,6-Dichlorophenylacetic acid → Sulfamic acid[2,6-dichlorophenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

HRID 1781464Notes

Reaction equation

HRID 1781464 reaction equation
CC(C1C=CC=C(C(C)C)C=1CC([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=O)C.C(C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.[Cl:49][C:50]1[CH:55]=[CH:54][CH:53]=[C:52]([Cl:56])[C:51]=1[CH2:57][C:58]([OH:60])=O>>[Cl:56][C:52]1[CH:53]=[CH:54][CH:55]=[C:50]([Cl:49])[C:51]=1[CH2:57][C:58]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:60]

Participants

4

Reactant 3

HCID 810582,6-Dichlorophenylacetic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 19046545Sulfamic acid[2,6-dichlorophenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with 2,6-dichlorophenylacetic acid, mp 203°-205° C.

Sources & evidence

ORD record
ord-9a8b83031a6a4f9d821ddccd1fc2046e
Source dataset
uspto-grants-1997_05
Patent number
US05633287

Reaction notes

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