2-Methoxyphenylacetic acid → Sulfamic acid[2-methoxyphenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

HRID 1781471Notes

Reaction equation

HRID 1781471 reaction equation
CC([C:4]1[CH:9]=[CH:8][CH:7]=[C:6](C(C)C)[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.C(C1C=CC=C(C(C)C)C=1C[C:46](O)=[O:47])(C)C.COC1C=CC=CC=1CC(O)=O>>[CH3:46][O:47][C:6]1[CH:7]=[CH:8][CH:9]=[CH:4][C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:31])[CH3:32])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][CH:21]=1)=[O:15]

Participants

4

Reactant 3

HCID 71342-Methoxyphenylacetic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 19046541Sulfamic acid[2-methoxyphenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with 2-methoxyphenylacetic acid, mp 159°-161° C.

Sources & evidence

ORD record
ord-88f9f92210aa4b5c86549ac389be44f2
Source dataset
uspto-grants-1997_05
Patent number
US05633287

Reaction notes

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