Hydrochloric Acid → HCID 19045712, compound

Participants

Reaction Steps

To a solution of 4,4-diphenyl-1-(3-nitrobenzylamino)-5-(tosylamino)pentane (0.17 g) in ethanol (10 ml) was added hydrochloric acid (0.1 ml) as well as 10% palladium-on-carbon (80 mg) and the mixture was subjected to catalytic hydrogenation at atmospheric temperature and pressure. The catalyst was then removed from the reaction mixture and the filtrate was concentrated to dryness. The group was dissolved in water and the solution was made basic with aqueous ammonia. The resulting precipitate was recovered by filtration, rinsed with water, and dried to provide the title compound (0.12 g) as light-tan powder.

Provenance & Evidence