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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1781963Erstellt: 25. Oktober 2026

4-(2-Anthryl)butanoic acid → Cbda 4-aba

https://huagongshe.com/reaction/1781963

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-(2-Anthryl)butanoic acidHCID 101380—
Edukt1,2,3,4-Cyclobutanetetracarboxylic dianhydrideHCID 107280—
LösungsmittelN-methyl-2-pyrrolidoneHCID 13387—
ProduktCbda 4-abaHCID 131727342—

Reaktionsschritte

19.22 g (0.098 mol) of CBDA, 9.77 g (0.08 mol) of 4-ABA and 5.85 g (0.02 mol) of DADOB were reacted in 197 g of NMP at room temperature for 5 hours to prepare a polyamic acid solution. The polymerization reaction proceeded easily and uniformly, and the molecular weights were measured in the same manner as in Preparation Example 1 and as a result, a solution of a polyamic acid having a number average molecular weight of 13,557 and a weight average molecular weight of 26,993 was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07498068B2
Quelldatensatzuspto-grants-2009_03
ORD IDord-d185d75b7569442fb2f6092f3d83f5ac
Quellennotizuspto-grants-2009_03