HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(2-Anthryl)butanoic acid → Cbda 4-aba
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(2-Anthryl)butanoic acid | HCID 101380 | — |
| Edukt | 1,2,3,4-Cyclobutanetetracarboxylic dianhydride | HCID 107280 | — |
| Lösungsmittel | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Produkt | Cbda 4-aba | HCID 131727342 | — |
Reaktionsschritte
19.22 g (0.098 mol) of CBDA, 9.77 g (0.08 mol) of 4-ABA and 5.85 g (0.02 mol) of DADOB were reacted in 197 g of NMP at room temperature for 5 hours to prepare a polyamic acid solution. The polymerization reaction proceeded easily and uniformly, and the molecular weights were measured in the same manner as in Preparation Example 1 and as a result, a solution of a polyamic acid having a number average molecular weight of 13,557 and a weight average molecular weight of 26,993 was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07498068B2 |
| Quelldatensatz | uspto-grants-2009_03 |
| ORD ID | ord-d185d75b7569442fb2f6092f3d83f5ac |
| Quellennotiz | uspto-grants-2009_03 |