HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl isocyanate → HCID 9846551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl isocyanate | HCID 160602 | — |
| Reactant | 4-amino-6-methoxy-7-(N-methylpiperidin-4-ylmethoxy)quinazoline | HCID 22243908 | — |
| Product | HCID 9846551 | HCID 9846551 | — |
Reaction Steps
Using an analogous procedure to that described in Example 3, phenethyl isocyanate was reacted with 4-amino-6methoxy-7-(N-methylpiperidin4ylmethoxy)quinazoline to give the title compound; NMR Spectrum: (CDCl3) 1.48 (m, 2H), 1.98 (m, 5H), 2.29 (s, 3H), 2.91 (m, 4H), 3.7 (q, 2H), 4.02 (d, 5H), 7.28 (m, partially obscured by CHCl3 peak), 8.47 (s, 1H), 8.65 (s, 1H), 10.1 (s, 1H); Mass Spectrum: M+H+ 450.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07498335B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-d6a5e42628a64b629fe82124f44b19d9 |
| Source note | uspto-grants-2009_03 |