HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Tricalcium Phosphate | HCID 24456 | — |
| Solvent | Water | HCID 962 | — |
| Product | Prop-2-enenitrile--ethenylbenzene (1/1) | HCID 62696 | — |
Reaction Steps
71 parts of styrene, 29 parts of acrylonitrile, 120 parts of deionized water and 0.17 parts of azobisisobutylonitrile (AIBN) were mixed. To the blend, 0.5 parts of tricalciumphosphate and 0.4 parts of t-dodecyl mercaptan chain transfer agent were added. The resultant solution was suspension polymerized at 75° C. for 5 hours. The resultant was washed, dehydrated and dried. Styrene-acrylonitrile copolymer (SAN) in powder state was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07498370B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-47b79b56e0894c9aa8116ee58ca7f4d3 |
| Source note | uspto-grants-2009_03 |