HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 3-Bromopropyl Ether → HCID 11598875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 3-Bromopropyl Ether | HCID 2776064 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11598875 | HCID 11598875 | 55.2% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0677 g, 0.231 mmol) and 3-bromopropyl phenylmethyl ether (0.070 mL, 0.396 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0663 g, 55.2%). EI-MS m/z 442(M+) Rt (2.23 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07498440B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-c74f7e464dd9443498d224e9f1ebe27f |
| Source note | uspto-grants-2009_03 |