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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1782444Generated: October 30, 2026

N-3-Bromopropylphthalimide → HCID 68959633, compound

https://huagongshe.com/reaction/1782444

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-3-BromopropylphthalimideHCID 21611—
Reactant1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanolHCID 23992385—
SolventAcetonitrileHCID 6342—
ProductHCID 68959633HCID 6895963382.4%

Reaction Steps

Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0861 g, 0.293 mmol) and 2-(3-bromopropyl)-1H-isoindole-1,3(2H)-dione (0.118 g, 0.440 mmol) in 2 CH3CN/3 CHCl3 (5.0 mL) were reacted to give the desired product (0.1319 g, 82.4%). EI-MS m/z 481(M+) Rt (1.90 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07498440B2
Source datasetuspto-grants-2009_03
ORD IDord-aba5bddc494a41f2b0c72f5c1b5aae04
Source noteuspto-grants-2009_03