HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-bromoethoxy)- → HCID 11713139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol | HCID 68865599 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11713139 | HCID 11713139 | 74.7% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol (0.0693 g, 0.227 mmol) and 2-bromoethyl phenyl ether (0.056 g, 0.279 mmol) in 1 MeOH/1 CHCl3 (3.0 mL) were reacted to give the desired product (0.0822 g, 74.7%). EI-MS m/z 426(M+) Rt (2.00 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07498440B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5faa1e540e0c42608c1ae0357ebc6da3 |
| Source note | uspto-grants-2009_03 |