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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1782455Generated: October 30, 2026

Benzene, (3-bromopropoxy)- → HCID 11591704, compound

https://huagongshe.com/reaction/1782455

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, (3-bromopropoxy)-HCID 68522—
ReactantHCID 68963321HCID 68963321—
SolventMethanolHCID 887—
ProductHCID 11591704HCID 1159170444.7%

Reaction Steps

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-3-thienyl)methanol (0.0808 g, 0.264 mmol) and 3-bromopropyl phenyl ether (0.070 mL, 0.444 mmol) in 2 MeOH/3 CHCl3/2 CH3CN (5.0 mL) were reacted to give the desired product (0.0613 g, 44.7%). EI-MS m/z 440(M+) Rt (2.05 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07498440B2
Source datasetuspto-grants-2009_03
ORD IDord-7c58e7719e2947228f7f1ba1f63e9b3e
Source noteuspto-grants-2009_03