Benzene, ((2-bromoethoxy)methyl)- → 4-{Hydroxy[bis(3-methylphenyl)]methyl}-1-{2-[(phenylmethyl)oxy]ethyl}-1-azoniabicyclo[2.2.2]octane bromide

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Reaction Steps

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4yl[bis(3-methylphenyl)]methanol (0.0496 g, 0.154 mmol) and 2-bromoethyl phenylmethyl ether (0.0364 mL, 0.230 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0091 g, 11.0%). EI-MS m/z 456(M+) Rt (2.20 min).

Provenance & Evidence