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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1782500Generated: October 29, 2026

1-(3-bromopropoxy)-2-methylbenzene → HCID 11613338, compound

https://huagongshe.com/reaction/1782500

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(3-bromopropoxy)-2-methylbenzeneHCID 1622574—
Reactant1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanolHCID 23992385—
SolventAcetonitrileHCID 6342—
ProductHCID 11613338HCID 1161333876.5%

Reaction Steps

Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442(M+) Rt (2.17 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07498440B2
Source datasetuspto-grants-2009_03
ORD IDord-1e12855d0143470ebc98d4e594fa9626
Source noteuspto-grants-2009_03