HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-bromopropoxy)-2-methylbenzene → HCID 11613338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-bromopropoxy)-2-methylbenzene | HCID 1622574 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11613338 | HCID 11613338 | 76.5% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0447 g, 0.152 mmol) and 3-bromopropyl 2-methylphenyl ether (0.0934 g, 0.407 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0586 g, 76.5%). EI-MS m/z 442(M+) Rt (2.17 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07498440B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-1e12855d0143470ebc98d4e594fa9626 |
| Source note | uspto-grants-2009_03 |