(R)-(+)-1-Phenylethyl isocyanate → HCID 68600725, compound

Participants

Reaction Steps

To a solution of 99 in DMF (0.75 mL) was added (R)-α-methylbenzylisocyanate (6 uL, 2.0 eq.) and TEA (8.5 uL, 3.0 eq.). The reaction was stirred under an atmosphere of argon for 20 hours. The reaction was then concentrated in vacuo and taken on to the next step without further purification.

Provenance & Evidence