HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzoylpiperazine → HCID 5495826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzoylpiperazine | HCID 762654 | — |
| Reactant | HCID 22893811 | HCID 22893811 | — |
| Product | HCID 5495826 | HCID 5495826 | — |
Reaction Steps
Precursor 5k, 1-benzoyl-4-[(7-chloro-6-azaindol-3-yl)-oxoacetyl]piperazine was prepared by the same method as Precursor 5a, starting from (7-chloro-6-azaindol-3-yl)-oxoacetic acid potassium salt, Precursor 4a, and 1-benzoylpiperazine. MS m/z: (M+H)+ calcd for C20H18ClN4O3: 397.11; found 396.97. HPLC retention time: 2.37 minutes (column F, gradient time=3 min, flow rate=4 ml/min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501420B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-d3019e452c0645ae8beeb8991dd46dc2 |
| Source note | uspto-grants-2009_03 |