4-Hydroxybenzylamine → HCID 135979597, compound

HRID 1784019Notes

Reaction equation

[CH2:1]([NH:3][C:4](=[O:26])[C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([NH:11][C:12]2[C:13]3[N:14]([N:23]=[CH:24][N:25]=3)[C:15]([C:18]3[CH:19]=[N:20][NH:21][CH:22]=3)=[CH:16][N:17]=2)[CH:6]=1)[CH3:2].[OH:27][C:28]1[CH:35]=[CH:34]C(CN)=[CH:30][CH:29]=1>>[OH:27][C:28]1[CH:35]=[CH:34][C:2]([CH2:1][NH:3][C:4](=[O:26])[C:5]2[CH:10]=[CH:9][CH:8]=[C:7]([NH:11][C:12]3[C:13]4[N:14]([N:23]=[CH:24][N:25]=4)[C:15]([C:18]4[CH:19]=[N:20][NH:21][CH:22]=4)=[CH:16][N:17]=3)[CH:6]=2)=[CH:30][CH:29]=1

Participants

Reactant 2

HCID 974724-Hydroxybenzylamine

HCID 135979621HCID 135979621, compound

Product 1

HCID 135979597HCID 135979597, compound

Procedure

This compound may be prepared using methods as described for Compound 129, using 4-hydroxybenzylamine in step 5. LCMS: Rt=0.98 min (100%), m/z (ESI) 427 (M+H)+.

Workup

customThis compound may be prepared

Sources & evidence

ORD record: ord-7c7545711ee54f68bf948b0658f08455
Source dataset: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07501411B2

Reaction notes

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