HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-fluoroaniline → HCID 11464172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-fluoroaniline | HCID 2782940 | — |
| Reactant | 2-chloro-9-methoxy-6,7-dihydro-4H-pyrimido[6,1-a]isoquinolin-4-one | HCID 57591093 | — |
| Product | HCID 11464172 | HCID 11464172 | — |
Reaction Steps
The title compound was prepared from 2-chloro-9-methoxy-6,7-dihydro-pyrimido[6,1-a]isoquinolin-4-one (4) and 2-bromo-6-fluoro-aniline as in Example 1 d. 1H-NMR (400 MHz, d6-DMSO) δ 9.26 (br, 1H), 7.72 (br, 1H), 7.57 (brd, 1H), 7.34 (br, 2H), 7.05-6.95 (2H), 6.37 (br, 1H), 3.94 (t, 2H), 3.84 (s, 3H) and 2.96 (t, 2H); MS (ESI) (M+H)+ 416, 418.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501512B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-b3272511036a47d788066056645698f7 |
| Source note | uspto-grants-2009_03 |