HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-N-phenyl-hydrazine → HCID 57591092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| Reactant | 2-chloro-9-methoxy-6,7-dihydro-4H-pyrimido[6,1-a]isoquinolin-4-one | HCID 57591093 | — |
| Product | HCID 57591092 | HCID 57591092 | — |
Reaction Steps
The title compound was prepared from 2-chloro-9-methoxy-6,7-dihydro-pyrimido[6,1-a]isoquinolin-4-one (4) and N-methyl-N-phenyl-hydrazine as in Example 1 d. 1H-NMR (400 MHz, d6-DMSO at 60° C.) δ 9.12 (br, 1H), 7.68 (d, 1H), 7.22 (t, 2H), 6.95-6.75 (5H), 6.24 (s, 1H), 3.96 (br, 2H), 3.82 (s, 3H), 3.16 (s, 3H) and 2.94 (t, 2H); MS (ESI) (M+H)+ 349.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501512B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-ba53c7a73ab848acbfbb41d961be87ed |
| Source note | uspto-grants-2009_03 |