HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 69049181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 7016243 | HCID 7016243 | — |
| Reactant | HCID 69049996 | HCID 69049996 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 69049181 | HCID 69049181 | — |
Reaction Steps
The sequence of reactions described in examples 53 to 57 was followed, however starting from 3,4-dimethoxyphenylglyoxal instead of 4-methoxyphenylglyoxal in the first step, and from methanol instead if isopropanol in the last step. This provided 2-amino-4-ethoxy-7-(3,4-dimethoxyphenyl) pteridine, a compound which was further characterized by its mass spectrum: 314 ([M+H]+, 100), 300 ([M+H-methane]+, 20).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501513B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-0613de76870a471481a9a851d9c28680 |
| Source note | uspto-grants-2009_03 |