HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbutanal → 5-Chloro-2-(2-methyl-butylamino)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbutanal | HCID 7284 | — |
| Reactant | 2-Amino-5-chlorobenzoic acid | HCID 12476 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Product | 5-Chloro-2-(2-methyl-butylamino)-benzoic acid | HCID 63538031 | — |
Reaction Steps
5-chloro-2-(2-methyl-butylamino)-benzoic acid was prepared from 2-amino-5-chloro-benzoic acid (23.31 mmol, 4.0 g) and 2-methylbutyraldehyde (23.31 mmol, 2.0 g) with sodium triacetoxyborohydride (96.62 mmol, 9.88 g) as per Procedure G (5.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07501538B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-3caad9211a7240708ab6639c302eda31 |
| Source note | uspto-grants-2009_03 |