HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 10435801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 91581604 | HCID 91581604 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10435801 | HCID 10435801 | — |
Reaction Steps
Phenylmethyl[3-[[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2-[[3[[(ethylamino)carbonyl]amino]phenyl]amino]pyrimidin-4-yl]amino]propyl]carbamate (145 mg) were stirred in a mixture of ethanol (10 ml) and hydrochloric acid (4 n; 1 ml) for 3 h at room temperature. Then halfconcentrated NaHCO3-solution and ethyl acetate were added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504410B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-f346902533df4fd98198e0b4e178b846 |
| Source note | uspto-grants-2009_03 |