4-Fluorobenzaldehyde → HCID 9869340, compound

Participants

Reaction Conditions

Reaction Steps

Tris(2-aminoethyl)amine (0.01 mol) and 4-fluoro-benzaldehyde (0.03 mol) were dissolved in MeOH (50 mL). After stirring at 25° C. for 15 h, NaBH4 (1.90 g, 0.05 mol) was added to the above solution at 0° C. The reaction mixture was stirred for 2 h at 25° C. It was then diluted with CH2Cl2 (100 mL) and ammonium chloride aqueous solution (10%, 70 mL).

Provenance & Evidence