HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69066824, compound → HCID 86600377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69066824 | HCID 69066824 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86600377 | HCID 86600377 | — |
Reaction Steps
The mixture of 1-{2-[2-(4-hydroxymethyl-phenyl)-1-methyl-ethylamino]-pyrimidin-4-yl}-8-phenyl-1,2,3,6-tetrahydro -pyrimido[1,2-a]pyrimidin-4-one (0.38 g, 0.81 mmol) and manganese dioxide (3.5 g, 40.5 mmol) in dichloromethane was stirred at room temperature for 3 h. The mixture was filtered off and concentrated to afford a white solid. M+1=467.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504403B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-6de1fbcc324e4549a960abe50ca5c371 |
| Source note | uspto-grants-2009_03 |