HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-hydroxyphenyl)boronic Acid → HCID 23654112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-hydroxyphenyl)boronic Acid | HCID 2734359 | — |
| Reactant | 4-Bromo-2-(5,6-dimethoxy-benzoimidazol-1-yl)-thiazole-5-carboxylic acid methyl ester | HCID 57595851 | — |
| Product | HCID 23654112 | HCID 23654112 | 6% |
Reaction Steps
In a similar manner as described for Example 26, 4-bromo-2-(5,6-dimethoxy-benzoimidazol-1-yl)-thiazole-5-carboxylic acid methyl ester (40 mg, 0.1 mmol) and 3-hydroxyphenylboronic acid (20.7 mg, 0.15 mmol) gave 2-(5,6-Dimethoxy-benzoimidazol-1-yl)-4-(3-hydroxy-phenyl)-thiazole-5-carboxylic acid (2.4 mg, 6%) as a white solid. MS m/z 398 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07504513B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5e3294a138ba401099617042607b4b46 |
| Source note | uspto-grants-2009_03 |