Benzocaine → HCID 22730540, compound

HRID 1785817Notes

Reaction equation

HRID 1785817 reaction equation
[CH:1]12[CH2:6][CH:5]1[C:4](=[O:7])O[C:2]2=[O:8].[NH2:9][C:10]1[CH:20]=[CH:19][C:13]([C:14]([O:16][CH2:17]C)=[O:15])=[CH:12][CH:11]=1.CC1(C)CC(=O)OC(=O)C1>>[O:7]=[C:4]1[N:9]([C:10]2[CH:11]=[CH:12][C:13]([C:14]([O:16][CH3:17])=[O:15])=[CH:19][CH:20]=2)[C:2](=[O:8])[CH:1]2[CH:5]1[CH2:6]2

Participants

4

Reactant 3

HCID 2337BenzocaineHCID 778133,3-Dimethylglutaric anhydrideHCID 27347213-Oxabicyclo(3.1.0)hexane-2,4-dione

Product 1

HCID 22730540HCID 22730540, compound

Procedure

The desired product was prepared by substituting methyl 4-aminobenzoate and 3-oxabicyclo(3.1.0)hexane-2,4-dione for ethyl 4-aminobenzoate and 3,3-dimethylglutaric anhydride, respectively, in Example 119A. MS (DCI) m/e 263 (M+NH4)+.

Sources & evidence

ORD record
ord-22d6046715d2402da5db918120b7e479
Source dataset
uspto-grants-2009_03
Patent number
US07504512B2

Reaction notes

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