Borane;tetrahydrofuran → HCID 22730070, compound

Participants

Reaction Steps

A solution of Example 266A (0.5 g, 2.82 mmol) in THF at room temperature was treated with 1M BH3.THF (15 mL), stirred for 18 hours, quenched with methanol (5 mL), and concentrated. The concentrate was treated with 2M HCl (50 mL) and concentrated. The the organic phase was dried (MgSO4), filtered, and concentrated to provide the desired product. MS (DCI(+)) m/e 182 (M+H)+.

Provenance & Evidence