Dimethyl(methylene)ammounium iodide → HCID 68406647, compound

Participants

Reaction Steps

As described for example 84b, 5-chloro-2-(4-methyl-imidazol-1-yl)-benzonitrile was reacted with Eschenmoser's salt in DMF for 16 h at 90° C. Evaporation of the solvent, aqueous workup and crystallization from ethyl acetate afforded the title compound as a white solid (yield: 17%). MS: m/e=275.1 [M+H]+.

Provenance & Evidence