HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(methylene)ammounium iodide → HCID 67549590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(methylene)ammounium iodide | HCID 2724133 | — |
| Reactant | HCID 68406876 | HCID 68406876 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67549590 | HCID 67549590 | 64% |
Reaction Steps
As described for example 84b, 5-methyl-2-(4-methyl-imidazol-1-yl)-benzonitrile was reacted with Eschenmoser's salt in DMF for 4 h at 90° C. Evaporation of the solvent, aqueous workup and chromatography afforded the title compound as an oil that solidified upon standing (yield: 64%). MS: m/e=255.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507729B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-c8ae426e86e24972b6e313864b0245ee |
| Source note | uspto-grants-2009_03 |