3-Acetylphenylboronic acid → HCID 18444551, compound

HRID 1786608Notes

Reaction equation

HRID 1786608 reaction equation
I[C:2]1[CH:18]=[CH:17][C:5]([O:6][CH2:7][C:8]2[CH:9]=[C:10]([C:14]([OH:16])=[O:15])[O:11][C:12]=2[CH3:13])=[CH:4][CH:3]=1.[C:19]([C:22]1[CH:23]=[C:24](B(O)O)[CH:25]=[CH:26][CH:27]=1)(=[O:21])[CH3:20]>>[C:19]([C:22]1[CH:27]=[C:26]([C:2]2[CH:18]=[CH:17][C:5]([O:6][CH2:7][C:8]3[CH:9]=[C:10]([C:14]([OH:16])=[O:15])[O:11][C:12]=3[CH3:13])=[CH:4][CH:3]=2)[CH:25]=[CH:24][CH:23]=1)(=[O:21])[CH3:20]

Participants

3

Reactant 2

HCID 27343103-Acetylphenylboronic acidHCID 184446544-(4-Iodo-phenoxymethyl)-5-methyl-furan-2-carboxylic acid

Product 1

HCID 18444551HCID 18444551, compound

Procedure

Compound (117) was prepared from compound (26) and (3-acetyl-phenyl)-boronic acid by adapting the procedure of Example 27B. LC/MS System B; Rt=1.69 mins, m/z (ES−) 349 (M−H for C21H18O5).

Sources & evidence

ORD record
ord-75029e6729194d0fb444b8fba2204342
Source dataset
uspto-grants-2009_03
Patent number
US07507754B2

Reaction notes

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