HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzenesulfonamide → N-[4-(biphenyl-4-ylaminomethyl)-5-methyl-furan-2-carbonyl]-2-methyl-benzenesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzenesulfonamide | HCID 6924 | — |
| Reactant | 4-(Biphenyl-4-ylaminomethyl)-5-methyl-furan-2-carboxylic acid | HCID 18444584 | — |
| Product | N-[4-(biphenyl-4-ylaminomethyl)-5-methyl-furan-2-carbonyl]-2-methyl-benzenesulphonamide | HCID 18444629 | — |
Reaction Steps
Compound (162) was prepared from compound (160) and 2-methyl-benzenesulphonamide by adapting the procedure of Example 38(f). LC/MS System D; Rt=10.39 mins, m/z (ES+)=461 (M+H for C26H24N2O4S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507754B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-d1a83f1c9f9749bfadc7b099ff1d977e |
| Source note | uspto-grants-2009_03 |