HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzenesulfonamide → N-(4-[(4'-Difluoromethoxy-biphenyl-4-ylamino)-methyl]-5-methyl-furan-2-carbonyl)-2-methyl-benzenesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzenesulfonamide | HCID 6924 | — |
| Reactant | 4-(4'-Difluoromethoxy-biphenyl-4-ylaminomethyl)-5-methyl-furan-2-carboxylic acid | HCID 18444564 | — |
| Product | N-(4-[(4'-Difluoromethoxy-biphenyl-4-ylamino)-methyl]-5-methyl-furan-2-carbonyl)-2-methyl-benzenesulphonamide | HCID 18444619 | — |
Reaction Steps
Compound (173) was prepared from compound (171) and 2-methyl-benzenesulphonamide by adapting the procedure of Example 38(f). LC/MS System D; Rt=10.63 mins, m/z (ES+)=527 (M+H for C27H24F2N2O5S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507754B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5258ab6b08134b9dac12a009777659f1 |
| Source note | uspto-grants-2009_03 |