HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 178433931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | 2,3-Dihydro-3-oxo-6-(4-pyridinyl)-4-pyridazinecarboxylic acid hydrazide | HCID 12790239 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178433931 | HCID 178433931 | — |
Reaction Steps
A mixture of 100 mg of 3-oxo-6-pyridin-4-yl-2,3-dihydro-pyridazine-4-carboxylic acid hydrazide, 130 mg thioacetamide, 87 mg triethylamine, 1 ml of pyridine and 5 ml of butanol is refluxed for 15 hours. After cooling and stirring at room temperature, a solid precipitated is collected by filtration, washed with cold isopropanol and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507734B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-9975cf0fb56142daa5f77fd28abbd97c |
| Source note | uspto-grants-2009_03 |