HCID 68707816, compound → HCID 23114273, compound

HRID 1787090Notes

Reaction equation

HRID 1787090 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:20])=[CH:16][C:17]([CH3:19])=[CH:18][C:13]=3[O:12][C:11]2=[O:21])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[OH:21][CH2:11][CH:10]([C:14]1[C:15]([CH3:20])=[CH:16][C:17]([CH3:19])=[CH:18][C:13]=1[OH:12])[C:7]1[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 68707816HCID 68707816, compound

Product 1

HCID 23114273HCID 23114273, compoundYield 93%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-4,6-dimethyl-1-benzofuran-2(3H)-one synthesized in Reference Example 4, the title compound was synthesized in the same manner as in Reference Example 8. Yield 93%. Melting point: 101-102° C. (ethyl acetate-hexane).

Workup

  1. customsynthesized in Reference Example 4

Sources & evidence

ORD record
ord-38992cda04e74b71804393b32ed6a00d
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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