4-Bromo-2-(2-hydroxy-1-(4-isopropylphenyl)ethyl)phenol → HCID 23114097, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5](O)=[C:4]([CH:9]([C:12]2[CH:17]=[CH:16][C:15]([CH:18]([CH3:20])[CH3:19])=[CH:14][CH:13]=2)[CH2:10][OH:11])[CH:3]=1>CO>[Br:1][C:2]1[CH:7]=[CH:6][C:5]2[O:11][CH2:10][CH:9]([C:12]3[CH:17]=[CH:16][C:15]([CH:18]([CH3:20])[CH3:19])=[CH:14][CH:13]=3)[C:4]=2[CH:3]=1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Using 4-bromo-2-(2-hydroxy-1-(4-isopropylphenyl)ethyl)phenol synthesized in Reference Example 11, the title compound was synthesized in the same manner as in Reference Example 13. Yield 62%. Melting point: 90-91° C. (methanol).
Workup
- customsynthesized in Reference Example 11
Sources & evidence
- ORD record
- ord-78f320e788624654b9df79edd1721746
- Source dataset
- uspto-grants-2009_03
- Patent number
- US07507841B2
Reaction notes
Loading…