HCID 23113857, compound → HCID 23114216, compound

HRID 1787106Notes

Reaction equation

HRID 1787106 reaction equation
C([NH:8][C:9]1[C:10]([CH3:23])=[C:11]([CH3:22])[C:12]2[O:16][C:15]([CH3:18])([CH3:17])[C:14](=[O:19])[C:13]=2[C:20]=1[CH3:21])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[NH2:8][C:9]1[C:10]([CH3:23])=[C:11]([CH3:22])[C:12]2[O:16][C:15]([CH3:17])([CH3:18])[C:14](=[O:19])[C:13]=2[C:20]=1[CH3:21]

Participants

3

Reactant 1

HCID 23113857HCID 23113857, compound

Product 1

HCID 23114216HCID 23114216, compoundYield 88%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 5-(benzylamino)-2,2,4,6,7-pentamethyl-1-benzofuran-3(2H)-one obtained in Reference Example 52, the title compound was synthesized in the same manner as in Reference Example 30. Yield 88%. Melting point: 92-93° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 52

Sources & evidence

ORD record
ord-d23742b8602f40599e8257802fb962e1
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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